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The bowl was mounted on a planetary ball mill (Fritsch, Pulverisette 7, classic line), and the speed was set to 500 rpm. The time was varied from 30 min to 24 h. After the milling, a bright green suspension was obtained, which was diluted with toluene (2 mL) and used asobtained or precipitated one time with acetonitrile ( mL, %, Aldrich).

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